The biomaterial scaffold is one of the most significant element in the subject of tissue engineering. This study may be providing an exhaustive synopsis of the main aspects of HA-AEMA-aerogel plus β-TCP. The characterizations of composites were performing with the analysis of mechanical properties, namely compressive strain, Young's modulus, swelling ability, structure and elemental analysis with a help of SEM and EDS. This demonstrates the potential of using those materials in combination to build in a scaffold with optimized qualities, hence, inspire future biomaterial development and applications.